Course Details
Subject {L-T-P / C} : CY5204 : Analytical Chemistry { 3-0-0 / 3}
Subject Nature : Theory
Coordinator : Prof. Rabindra Kumar Behera
Syllabus
Errors and evaluation: Errors, Determinant, constant and indeterminate. Accuracy and precision,
Distribution of random errors. Average derivation and standard derivation, variance and confidance
limit. Significance of figures and computation rules. Least square method. Methods of sampling:
samples size. Techniques of sampling of gases, fluid, solids, and particulates, Chromatographic
methods: General principle, classification of chromatographic methods. Nature of partition forces.
Chromatographic behavior of solutes. Column efficiency and resolution. Gas Chromatography, Thin
layer chromatography, Column chromatography, High pressure liquid chromatography, Ion
exchanges chromatography: Instrumentation, detector, optimization of experimental conditions
and analytical application, Electroanalytical Techniques: Basic principles, instrumentation and
analytical application pH – metry, potentiometry,conductometry,coulometry, polarography,
voltammetry, Amperometry and ion selective electrodes, Thermal method of analysis,
Thermogravimetriy [TG], differential thermal analysis [DTA], differential Scanning calorimetric [DCS],
Thermometric titrations, Basic principle, Instrumentation and analytical application, Atomic
Spectroscopic Techniques: Atomic absorption (flame,graphite furnace,hydride generation and cold
vapour) and atomic emission (flame,plasma,spark and arc) spectroscopy, Radioanalytical
Techniques: Neutron Activation analysis, isotope dilution analysis, radiometric titrations
Course Objectives
- To educate different types of analytical techniques exercised in chemistry.
Course Outcomes
1) Students will be familiar of different types of analytical techniques exercised in chemistry. <br />2) Students will be able to learn both theoretical and instrumental aspects of various detection <br />processes.
Essential Reading
- LR. Shyder and C.H.Harvath, An Introduction to separation Science, Wiley Interscience , 2010
- H.H . Willard, L.L. Mirrit, J.A. Dean, Instrumental Methods of analysis, CBS , 2014
Supplementary Reading
- B. K. Sharma, Analytical Chemistry, Krishna’s Educational Publishers , 2012
- G.W. Ewing, Instrumental Methods of Analysis, McGraw-Hill College 5th edition , 2009