Course Details
Subject {L-T-P / C} : MM6572 : Experimental Techniques in Materials Engineering Laboratory { 0-0-3 / 2}
Subject Nature : Practical
Coordinator : Prof. Santosh Kumar Sahoo
Syllabus
Analysis of X-ray diffraction in cubic (FCC and BCC) metals. Analysis of X-ray diffraction in hexagonal (HCP) metals. Study of unknown samples using X-ray diffractometer. Determination of residual stress, residual strain and grain size of deformed metals. Study of Scanning Electron Microscope, and EDS analysis of metals/alloys. Thermal analysis by DTA, TGA, DSC on metallic sample.
Course Objectives
- 1. Crystallographic analysis through XRD.
- 2. Microstructural characterization through SEM and TEM.
- 3. Elemental analysis through EDS and WDS.
- 4. Characterization of phase transformation through thermal analysis techniques.
Course Outcomes
CO1: Analysis of different phases in a material. <br />CO2: Analysis of crystallite size (grain size) and lattice strain in a material. <br />CO3: Analysis of residual stresses in a material. <br />CO4: Analysis of chemical composition of a material. <br />CO5: Analysis of phase transformation in a material.
Essential Reading
- .1. B. D. Cullity and S. R. Stock, Elements of X-ray Diffraction, Prentice-Hall, New Jersy, 2001., ., . , .
- .2. C. Suryanarayana and M. Grant Norton, X-ray Diffraction A Practical Approach, Springer, New York, 1998., ., . , .
Supplementary Reading
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Journal and Conferences
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