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Phenyl Trimethyl Ammonium Tribromide Mediated Robust One-pot Synthesis of Spiro-oxacycles– An Economic Way Out–Stereoselective Synthesis of Oxaspirohexacyclodieneones, Debayan Sarkar*, Manoj Kumar Ghosh, Nilendri Rout, Department of Chemistry

T
he manuscript entails the first recognition of Phenyl Trimethyl Ammonium Tribromide (PTAB) as an effective reagent for spiro-cyclizations proceeding via oxidative dearomatization.The experiment exhibits economic, metal and ligand free one-pot accomplishment of these significant
transformations. The described protocol presents the first generalised methodology of spiro-oxacycle synthesis which can be applied towards various directions. A stereoselective synthesis of oxa-spirocyclooxadieneones has been accomplished. More in Organic & Biomolecular Chemistry,RSC, 2016, DOI: 10.1039/C6OB01116K. (List of Research)

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PI: Dr. Snehanshu Pal
Sponsor: Naval Research Board (NRB), DRDO, Government of India
 
Development of KW Class Cryogenic Helium Turboexpander .......
PI: Prof. Ranjit Kumar Sahoo
Sponsor: BRNS, Govt. of India
 
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