National Institute of Technology Rourkela

राष्ट्रीय प्रौद्योगिकी संस्थान राउरकेला

ଜାତୀୟ ପ୍ରଯୁକ୍ତି ପ୍ରତିଷ୍ଠାନ ରାଉରକେଲା

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Syllabus

Course Details

Subject {L-T-P / C} : PH6573 : Semiconductor Materials Characterization Laboratory { 0-0-3 / 2}

Subject Nature : Practical

Coordinator : Jyoti Prakash Kar

Syllabus

Module 1 :

To estimate the crystal structure, and lattice parameters of a given semiconducting material using X-ray diffraction technique. [Software: Rietveld refinement by FullProf software]

Module 2 :

To determine (i) the composition of a semiconducting material surfaces (elemental identification and (ii) the chemical state of polyvalent ions by measuring the binding energies of elements

Module 3 :

To study the chemical structure, phase, polymorphism, crystallinity, and molecular interactions of a given semiconducting material using Raman spectroscopy

Module 4 :

To (i) study surface/interface morphology using scanning electron microscopy (SEM) high-resolution images, (ii) determine elemental composition employing energy dispersive X-ray spectroscopy (EDS)

Module 5 :

To measures surface topography at the nanometer scale using atomic force microscopy (AFM)

Module 6 :

To visualize, inspect, quantify, and validate scientific image data using ImageJ software

Module 7 :

To measure the work function and surface potential of a given semiconducting materials using Kelvin probe force microscopy

Module 8 :

To calculate the charge density in a metal-oxide-semiconductor (MOS) structure using capacitance-voltage (C-V) measurements

Module 9 :

To study the current-voltage (I-V) characteristics of a metal-oxide-semiconductor (MOS) structure

Module 10 :

To calculate the mobility, carrier concentration of given semiconductor by Hall probe measurement system

Module 11 :

Current-time (I-t) measurements of photodetector and chemical sensors

Course Objective

1 .

To impart knowledge on analysis of experimental data, interpreting results, and understanding how different characterization methods correlate with material properties

2 .

Fundamental electronic, optical, and structural properties of semiconductor materials through practical experiments

3 .

Execution, and troubleshooting of experiments related to semiconductor materials and devices

4 .

Advanced research and development activities in the field of semiconductor technology by providing a solid foundation in characterization techniques

Course Outcome

1 .

At the end of course, students will be able to develop strong research skills, including the ability to design experiments, solve practical problems, and conduct scientific investigations with a clear understanding of the methodologies involved

2 .

Troubleshoot and adapt experimental procedures to address challenges and improve accuracy

3 .

Execute experiments meticulously, document procedures, and ensure data integrity

Essential Reading

1 .

Laboratory Manual, Laboratory Manual, Laboratory Manual , Laboratory Manual

2 .

Y. Leng, Materials Characterization: Introduction to Microscopic and Spectroscopic Methods, Wiley-VCH , (2013)

Supplementary Reading

1 .

C. Suryanarayana, M. Grant Norton, X-Ray Diffraction: A Practical Approach, Springer , (2014)

Journal and Conferences

1 .