National Institute of Technology Rourkela

राष्ट्रीय प्रौद्योगिकी संस्थान राउरकेला

ଜାତୀୟ ପ୍ରଯୁକ୍ତି ପ୍ରତିଷ୍ଠାନ ରାଉରକେଲା

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Syllabus

Course Details

Subject {L-T-P / C} : CY2171 : Functional Group Identification Laboratory { 0-0-3 / 2}

Subject Nature : Practical

Coordinator : Sabita Patel

Syllabus

Module 1 :

Detection of elements (N, S, Halogens) in organic Compounds, Detection of functional groups: amine, amide, alcohol, phenol, nitro compounds, carboxylic acid, aldehyde, ketone, unsaturation, Monosaccarides etc., Derivative preparation (amide, acid, anilide, ester, picrate, hydrazone, semicarbazone, 2, 4-DNP, Osazone etc.), Crystallization of derivatives and characterization using melting point comparison.

Course Objective

1 .

To get practical skills to perform relevant chemical tests, interpretation of results, and understanding the underlying principles.

2 .

To relate the knowledge gained in theory to practical laboratory experiments

Course Outcome

1 .

CO1: Students will gain basic level scientific and practical understanding of chemistry of organic functional group.
CO2: Students will learn practical skills to perform relevant chemical tests, interpretation of results to deduce the presence or absence of specific functional groups and understanding the underlying principles.
CO3: 5. Students will learn basic laboratory techniques, such as handling chemicals, using glassware, and performing simple reactions.

Essential Reading

1 .

V K Ahluwalia and R Aggarwal, Comprehensive practical organic chemistry, University Press , 2000

2 .

Brian S. Furniss, Vogel’s Text Book of Practical Organic Chemistry, ELBS Longman , 5th edition, 1996.

Supplementary Reading

1 .

A. K. Nad, B. Mahapatra, A Ghosal, An advance course in practical chemistry, New central book agency(P) ltd. , 3rd edition, 2007.

2 .

Donald L. Pavia, Gary M. Lampman, George S. Kriz, James F. Engel, Organic Chemistry: A Lab Manual, Cengage Learning , 1st Edition, 2009