National Institute of Technology Rourkela

राष्ट्रीय प्रौद्योगिकी संस्थान राउरकेला

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Syllabus

Course Details

Subject {L-T-P / C} : CY2702 : Basic Physical Chemistry Laboratory - I { 0-0-2 / 1}

Subject Nature : Practical

Coordinator : Usharani Subuddhi

Syllabus

Module 1 :

1. Determination of Order for the Persulphate-Iodide Reaction
2. Determination of the rate constant of hydrolysis of an ester in aqueous acidic medium.
3. Conductometric titration of a mixture of strong and weak acid with a strong base
4. pH metric titration of a mixture of strong and weak acid with a strong base
5. Study of the distribution equilibrium of iodine in water/tolune.
6. Adsorption charatertistics of acetic acid on charcoal
7. Verification of Beer-Lambert law.
8. Ionization constant of a weak acid (acetic acid).
9. Solubility of a sparingly soluble salt.
10. Determination of pKa values of Orhophosphoric acid using pH Meter

Course Objective

1 .

These experiments are intended to acquaint the students with the practice of experimental physical chemistry

2 .

The students will receive adequate exposure so that they can independently handle and interpret data from basic instruments used in physical chemistry

Course Outcome

1 .

Students are expected to understand the interconnection between experimental foundation and underlying theoretical principles and to develop laboratory skills and get familiar with a variety of physico-chemical measurement techniques

Essential Reading

1 .

R. C. Das and B. Behera, Experimental Physical Chemistry, Tata McGraw Hill

Supplementary Reading

1 .

B. Viswanathan and P. S. Raghavan, Practical Physical Chemistry, Viva Books