Syllabus

Electromagnetic radiations: Types of molecular energy and molecular spectroscopy(1 hour). NMR Spectroscopy: Basic principles (2 hours), Chemical shift (2 hours), Spin-Spin Coupling (2 hours), Coupling Constant (2 hours), NOE, 13C NMR (6 hours), 19F, 31P NMR (2 hours), DEPT NMR (2 hour), heteronuclear coupling (2 hour), Pulse NMR spectroscopy and techniques (2 hours), relaxation time and their importance (2 hours), 2D NMR spectroscopy: COSY, NOESY, HMQC, HMBC (7 hours) Problem involving these techniques for structural determination and other applications (8 hours).

To introduce NMR Spectroscopy, a vital method of characterization of organic molecules.

Problem solving by NMR spectroscopy

To give details of different nuclei/atom characterisation by NMR Spectroscopy.

To train students for phrmaceutical jobs and research in any field dealing with organic molecules.

1) The students will able to understand the basic concept of NMR spectroscopy used for the analysis of organic compounds.
2) Detailed discussions on principles, instrumentation and applications of these techniques will be carried out.
3) Information about application and importance of 2D NMR spectroscopic methods, would help in complex molecule characterization.
4) The students would learn the elucidation of structures from the NMR spectrum (Both 1D and 2D)
5) Different aspects of NMR spectroscopy , besides structure elucidation, would be detailed.

D. C. Pavia, G. M. Lampman, G. S. Kriz, Introduction to Spectroscopy, THOMSON

J. Mohan, Organic Spectroscopy, Narosa Publishing House

B. H. Williams, I. Flemming, Spectroscopy Methods in Organic Chemistry, McGraw Hill

Bessler and Silverstein, Spectroscopy of Organic Compounds, JOHN WILEY