National Institute of Technology Rourkela

राष्ट्रीय प्रौद्योगिकी संस्थान राउरकेला

ଜାତୀୟ ପ୍ରଯୁକ୍ତି ପ୍ରତିଷ୍ଠାନ ରାଉରକେଲା

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Syllabus

Course Details

Subject {L-T-P / C} : CY4702 : Inorganic Chemistry Laboratory { 0-0-3 / 2}

Subject Nature : Practical

Coordinator : Saurav Chatterjee

Syllabus

Module 1 :

Semimicro qualitative analysis of cations, Step by step Group-test analysis (anions are excluded) and the identification of cations in a given sample. Group 1-5 cations confirmatory test in unknown sample. Identification and Removal of interfering ions like phosphate. Treatment of Insoluble salts or residue for analysis. Synthesis of inorganic / organometallic compounds . Characterization and property measurements of inorganic compounds. Exposure to various spectroscopic characterization techniques.

Course Objective

1 .

To learn qualitative analysis and identification of various cations

2 .

To learn the separation procedures using grout test analysis and different confirmatory test for cations ,

3 .

To Learn step by step Group test analysis including removal of interfering ions

4 .

To understand the estimation techniques and spectroscopic analysis of inorganic salts/compounds.

Course Outcome

1 .

1. The students will have hands-on experience on techniques used for qualitative analysis using group test of cations.
2. Learn different quantitative estimations of inorganic compounds.
3. Understand the chemistry behind the qualitative analysis and will be able to estimate cations in a mixture sample.
4. Will be capable to undergo cation identification and estimation in real time water sample.

Essential Reading

1 .

A. I. Vogel, Qualitative Inorganic Analysis, Pearson, India

Supplementary Reading

1 .

A. I. Vogel, John Bassett, Vogel's textbook of quantitative inorganic analysis: including elementary instrumental analysis, Longman