National Institute of Technology Rourkela

राष्ट्रीय प्रौद्योगिकी संस्थान राउरकेला

ଜାତୀୟ ପ୍ରଯୁକ୍ତି ପ୍ରତିଷ୍ଠାନ ରାଉରକେଲା

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Syllabus

Course Details

Subject {L-T-P / C} : CY4705 : Materials Synthesis Laboratory { 0-0-3 / 2}

Subject Nature : Practical

Coordinator : Sasmita Mohapatra

Syllabus

Module 1 :

Synthesis of oxides, sulfides, solid solutions, nanomaterials, as well as intercalation compounds using various synthetic methods such as solid state reaction, combustion, sol-gel, coprecipitation, hydrothermal, intercalation/deintercalation and organometallic precursor routes.
Characterization of the synthesized materials for determination of their structure, composition, morphology and physicochemical properties using XRD, IR, SEM, PPMS and temperature programmed method.

Course Objective

1 .

To train students on basic methods for synthesis of materials

2 .

To provide hands-on experience in the preparation, characterization, and analysis of various materials

Course Outcome

1 .

1. Students will understand the principles governing material synthesis, such as nucleation, growth, and phase transformations.
2. Students will learn various synthesis methods such as sol-gel, hydrothermal, solid-state, co-precipitation
3. Students will gain practical skills in handling raw materials and precursors for synthesis.

Essential Reading

1 .

A. R. West, Solid state chemistry and its applications, Wiley Student addition (John Wiley & Sons)